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#168 From: "Geo>K0FF" <GEOelectronics@...>
Date: Sat Jul 5, 2008 5:54 pm
Subject: Calibrating a Survey Meter> A Tutorial by Geo
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Calibrating a Survey Meter> A Tutorial by Geo

 

STEP 1:

Check the instrument and probe for contamination. a frisker (pancake probe) should be used so that all types of

contamination may be detected.

 

Step 2: Check for mechanical meter zero and overall mechanical condition of the unit, including battery compartment and terminal corrosion.

 

Step 3: Determine the level and type of calibration needed. First time use of an instrument can proceed to as-left or final calibration immediately. If the instrument has been in service for a time and in for periodic calibration, AS-FOUND readings must first be taken and recorded before any adjustments are made. This will leave a paper trail for documents that may have had the meter in question used for measurements in the recent past.

 

Step 4: Measuring the As-Found High Voltage. Connect the meter to a super high impedance Voltmeter of at least 1000 Meg Ohms input impedance. The HV meter in a Ludlum Model 500 Pulser meets this requirement. An ordinary DVM is NOT acceptable. Their low 10 MegOhm impedance will drag down the meter's HV and produce an erroneous reading. ONLY use a super high impedance meter, or an approved adaptor for a regular DVM. Record the As-Found HV reading and the type of instrument used to measure it.

  

 

The following discussion concerns the factors involved in calibrating a handheld radiation detector system "Survey Meter", such as the Ludlum Model 3.

Some of the information may also applicable to other detection systems.

 

Exposure Rate Calibration vs. Electronic CPM (Pulser) Calibration.

Exposure Rate Calibration is done in a lab with a Radiation Range. This is usually several milliCuries of Cs-137, enough to flood the entire instrument with a uniform radiation field in the exposure ranges covered by that particular probe-meter combination. Ranges are set up with adjustable attenuators and calibrated distances so that various exposure rates may be employed. All of the parameters for that particular probe, such as input sensitivity, HV operating point, WINDOW adjustment, and deadtime are specific to that probe alone.

Once a calibration is completed with this method, the probe and meter are married together as a unit and will be tagged as such so that no other probe will be used with that meter.

Never forget that most probes/meters will only read exposure rates accurately when exposed to Cs-137. Other isotopes will display more or less than the actual dose rate, depending on the energy response of the probe. See the tutorial entitled: "Radiation Probes and Their Dial Scales"

 

Electronic or Pulser Calibration. When more than one probe is to be used with a meter, electronic CPM calibration is required. Never forget that a meter scale with dose rate will only be accurate for a specific type of probe. Each different probe will have a particular CPM per mR/H factor that is only good for that one type of probe. See the tutorial entitled: "Radiation Probes and Their Dial Scales"

 

Next, determine the input sensitivity of the meter unit. Ludlum Model 3's are fixed, and specified for 40 mV +/- 10 mV.  Set the Pulser output Voltage adjustment to zero. There will be not reading on the meter unit under test at this point. Adjust the Pulser CPM for mid scale for the range selected. Now slowly increase the output Voltage until the meter under test just starts to respond. Carefully increase or decrease the Pulser output Voltage until the meter is reading steadily and shows 80% of the Pulser's reading. Record this level as the " Input Sensitivity".

If AS-Found readings need to be recorded, adjust the Pulser on each range to read 20% and then 80% of full scale on that range, then record the CPM required to get that reading.

Example: A dial might be 6,000 CPM full scale. Adjust the Pulser so that the needle goes to 1200 CPM, and record the Pulser CPM required to achieve this. Ideally it will be 1200 CPM. Record the actual Pulser CPM and the CPM read on the meter: Pulser>1300 CPM/ Meter> 1200 CPM. Do this for 20% and 80% of each range step,

 

 Use the Ludlum 500 or equivalent Pulser to generate CPM rates that equal 20% and 80% of each range setting. Since there is only one calibration control for each range,

set the 80% mark first then check the 20% mark. If it is within manufacturer's specifications, that range is then calibrated. If the both areas of the scale are not within specifications, an intermediate setting of the calibration control may be found to balance both reading within specifications. If readings can't be adjusted properly, fail the instrument and send it to the repair facility. 

 

Testing the PROBE.

Many types of radiation probes exist. The types we are concerned with for use with Survey Meters all produce pulses, as contrasted to ion-chambers that usually operate in the current mode.

Height or amplitude of the pulses generated by the probe are very different depending on the technology employed, and in all cases, the operating parameters for that probe must be matched by the parameters of the meter. A meter set up for a proportional probe will not be interchangeable with a GM probe.

 

Some typical operating Voltage requirements and pulse heights;

GM Tube of all descriptions: 450, 700 or 900V, pulse of several Volts. No energy information contained in the pulse. All pulses the same.

Scintillator: 600 to 1200V, pulse of 10 mV to 500 or more mV. Pulse height = energy deposited. Especially in NaI(Tl)

Proportional Probe: 1000-2000V, pulse of 2 mV and up, depending on radiation type.

 

Probes with less than 1 mV output pulses will require charge-coupled amplifiers in the meter, as opposed to the common voltage amplifiers used in most Survey Meters. Charge coupled amplifiers require an adaptor to measure with the Pulser.

 

PLATEAU and Operating Voltage. Typical operating Voltages are listed in the probe's instruction manual. To make sure the probe is within specifications, a Plateau should be performed.

 

Set the meter up with normal parameters for the probe type being tested, but turn the HV all the way down. Connect the probe to the meter and expose the probe to a radiation source (test disc). In crease the HV until the probe just starts to count, record this Voltage as the "Start". Further increase the HV until there is noticed a SHARP increase in counts, record this Voltage and label as "Knee or “Threshold of Plateau “", continue increasing HV and notice that the counts increase very slowly in this "plateau" area, and at some point they level off, hardly increasing at all with higher Voltages. Label this Voltage as "End". If HV is increase above this point, total discharge may take place, damaging the tube. Select the OPERATING POINT as about 25-50V above the "Knee".

 

http://www.ortec-online.com/application-notes/an34/exp02.pdf

 

Scintillator Operating Points are determined in a similar manner for general-purpose use. Specialized setting may be required when energy determination is the goal.

 

Once the operating point is determined and the HV set for that level, the probe can be tested for efficiency using NIST calibrated test discs. Various types of radiation and energy levels will be employed, covering all the different regions that the probe is capable of detecting. These isotopes are commonly used:

 

Beta:

C-14           156 keV Max      44-9 2 Pi efficiency = 10%

Sr-90/Y-90  2.28 MeV Max   44-9 2Pi efficiency =  45%

Tc-99            293 keV Max      44-9 2Pi efficiency = 38%       

P-32             1.71 MeV Max   44-9 2Pi efficiency = 65%                                                                   

 

Alpha

Pu-239           5 MeV               44-9 2Pi efficiency = 30%

 

Many GM probes are designed to be used at 900V, making them fully interchangeable on a survey meter set to 900V. NEVER forget that ONLY the CPM scale is universal and all mR/H sales are only for one type of probe.

Ludlum also specs 900V as the typical operating Voltage for many of their scintillator probes, making them somewhat interchangeable with many of their GM probes.

 

IDEALLY, a probe and a meter with the proper scale on the dial are set up using a radiation range, and that combination of meter and probe are tagged so as to be married together as a unit from that time forward.

 


#167 From: "Geo>K0FF" <GEOelectronics@...>
Date: Sat Jul 5, 2008 1:35 am
Subject: Relationship of probes and dial scales explained
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Radiation Detection Probes and Their Dial Scales> A Tutorial by Geo

 

Pay attention to the Gamma Sensitivity numbers in the specification sheets and charts. This figure gives a clue as to how sensitive a certain tube is compared to another tube or probe. The number indicates how many pulses you would get from a uniform flux of Cs-137, in counts per minute/per mR/H. Each probe must use a dial scale that is correctly delineated for the CPM/mR/H of that probe. Only LUDLUM MEASUREMENTS makes dial scales that are easily changed to match their respective probes. NOTE: The mR/H scale is ONLY accurate when measuring Cs-137, OR when using an energy compensated probe (44-38).

                       
For all probes except the few specifically labeled “Energy Compensated”, the other factor is Gamma Energy Response> different tubes and probes  will respond to varying energy levels according mainly to he construction materials used, and volume and pressure of fill gas or crystal (size of probe). In general, Low Energy Gammas (LEG) must be of sufficient strength (meaning energy level, not number of disintegrations) to penetrate the housing material. A Z number is used to indicate density of any material, based on atomic makeup. Some probes utilize LOW Z windows to allow in extra low energy rays and particles.

Once inside the tube, lower energy Gammas are much more likely to cause an interaction, and therefore be counted. At some point as the energy level increases, the ray will simply pass out of the tube and not be counted. These facts account for the whipsaw shape of the energy response curves of all GM tubes. External filtering may be applied to compensate for this non linear effect, resulting in a probe that is called" energy compensated". Be aware that this procedure knocks all the response down to the lowest level, and that although now nearly perfectly linear, such a probe will give lower reading than you may be used to from the more common "energy dependant" probes.

Making a rough estimate of activity may be found by applying this formula:
@1 meter 1Ci= .381 R

where 1uCi=10^-6 Ci

and using the inverse squared law:
@ 1/2 meter = X4
@1/4 meter = X 16
@ 1/8 meter= X64
@ 1/16 meter = X256
etc.

1 uCi is always equal to 3.7 X 10^4 DPS (disintegrations per second) or 2.22 X10^6 DPM no matter what type of radiation is involved.
http://www.sizes.com/units/curie.htm
http://www.radcon.arizona.edu/training/RSPC-CH.pdf

When the term 4Pi is used, it refers to disintegrations in all directions, as in a sphere. Most probes can only see from one
direction and as such are 2Pi (1/2 of a sphere). GEOMETRY is the term used to indicate the area that the radiation fills in relation to the probe. Technically it is the angle subtended by the probe.
Best geometry is achieved if the probe is 10X it's own diameter away from the source.
4Pi or near 4Pi can be achieved with hollow probes (as in WELL probes) where the radioactive sample is placed inside. Liquid scintillators are also 4Pi, as the sample is inside the liquid.

 
 



   

0-6.6k cpm; 0-2 mR/hr
For Model 44-9; 44-9-18;
44-40; 44-88; 44-89; 44-94

 

 

 

 

 

 

 

 

   

202-330
0-4k cpm; 0-2 mR/hr
For Model 44-7
 

 

 

202-241
0-2 mR/hr; 0-2.4k cpm
For Model 44-6; 44-38

 

 
 
 

 202-654
0-50
mR/hr; 0 - 8.5k cpm
For Model 44-2

 

 

 

 

 

202-717
0-5
mR/hr
For Model 44-10

 

 

 

 

 

 

202-212
0-5
mR/hr; 0-3500 cpm
For Model 44-3(I-125)

 

LOW ENERGY GAMMA (LEG) Probes have a thin crystal, making them more like"non-high energy detectors".

Since low energy Gammas and X-Rays are absorbed in the first 1/100th of an inch in NaI(Tl), there is no need to make the crystal any thicker than that.

Without a thick crystal, high energy rays are not well absorbed, therefore add little to the desired signal.

In addition most LEG probes incorporate some sort of thin entrance window, making it easier for the LEG to penetrate into the crystal.

 

 

 

 

 

 

 

George Dowell

New London Nucleonics Laboratory

Copyright © Viscom Inc. 2007

The treatise may under no circumstances be resold or redistributed in either printed, electronic,

or any other forms, without prior written permission from the author.

Comments, criticism and questions will be appreciated and may be directed to

the author by email to GEOelectronics@...          


#166 From: "Geo>K0FF" <GEOelectronics@...>
Date: Fri Jul 4, 2008 5:35 pm
Subject: CDV Q+A Goes here
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#165 From: "Geo>K0FF" <GEOelectronics@...>
Date: Fri Jul 4, 2008 5:14 pm
Subject: Q+A goes here:
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#163 From: "jasonburry" <jasonburry@...>
Date: Fri May 30, 2008 7:01 pm
Subject: Nuclear Decay Processes Explained, and where did those particles come from?
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Hello Folks!

This is an explanation of how nuclear decay happens, and where the
alpha, beta and gammas we all love to measure come from.

For all intents and purposes, nuclear decay is always by a particle
exchange mechanism. The nucleus either emits or captures a partial.
Generally, this is either by:

1) Alpha decay - the nucleus undergoes what amounts to a very uneven
spontaneous nuclear fission, and emits a He nucleus (2 neutrons, and
2 protons). It steps 2 elements down the periodic table, and loses 4
mass units. This is the alpha decay we all talk about, though I've
read that many other forms of alpha decay do exist in some more
exotic isotopes, where the emitted "alpha" is other than a helium
nucleus, but is some other light nucleus. We're pretty unlikely to
encounter this in the home lab, methinks.... In my mind, any
spontanious fission is actually an exotic alpha decay.

2) Beta- decay - the nucleus emits an electron, and thus the nucleus
charge goes +1, and the nucleus "climbs" one step up the periodic
table. The beta (electron) is emitted by a neutron in the nucleus,
and in doing so, the neutron becomes a proton. The mass is
essentially the same, but the charge is now different

3) Beta+ decay - The nucleus emits a positron (Anti-matter in the
Home Lab!), or a positively charged "electron". Na22 is one such
isotope. In this case, the nucleus charge goes -1, but again the
mass is essentially the same.

4) Electron Capture (EC) - another rather exotic process, basically
the reverse of beta decay. A proton in the nucleus absorbs an
electron and becomes a neutron. Mass is the same, charge is -1, as
in beta+ decay.

All these decay modes may leave the nucleus in an upset state. Like
a Jenga tower with bricks removed from below, it's unstable. As
it "collapses" to a more stable state (the jenga tower sees this as
a pile of rubble), it has to release energy. That energy is
typically a Gamma Ray, a high energy photon. Gammas are simply a
result of the new nucleus relaxing and coming to terms with its new
form.

In the case of the natural decay chains, each step is by one of the
processes above (generally B- or Alpha). After each step, a gamma
may be emitted as the new nucleus relaxes. Decay chain charts don't
always list these gammas because they're not relevant to the actual
changes. But, if you look at each isotope in the decay chain, look
it up in Wiki or whatever you like, you'll see what gammas it
typically emits in its decay.

As an aside, the difference between Gammas and X rays: To your
geiger counter, there is NO DIFFERENCE! The only difference is that
the gamma is made by a nucleus performing an energy balancing act
(as I described above), while an X-ray is the result of the atom's
electrons moving to a lower energy state. So Gammas come from the
nucleus, and are a nuclear event, while Xrays are from the electron
cloud, and are an electronic event.

Hope it helps...

J

#162 From: "Geo>K0FF" <GEOelectronics@...>
Date: Thu May 22, 2008 12:39 am
Subject: Gamma Energy Response Exercise
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Q:
Take 3 imaginary isotopes.
 
#1 has a peak at 100 keV only, # 2 has a peak at 662 keV only and #3 has a single peak at 3 MeV.
 
Each sample has the same number of photons output per minute, let's call it 1000 to make it ultra simple.
 
What counts would be expected in peak 100 keV, 662 keV and 3 MeV respectively, assuming a 60 second count time.
 
 
 
Givens:
All samples are the same size, density and distance form the probe.
The geometry of all samples is equal and the probe housing passes all energies equally well.
 
A:
The way to answer this question would be:
 
100 keV = 500% N
662 keV= 100% N
3 MeV = 20% N
 
Whatever number of counts would be in the 662 keV peak would equal 100 %. The 100 keV peak would have 5 times that may counts while the 3 MeV peak would contain 25% as many counts.
 
Per this chart:
 
Notice that the chart is centered on 662 keV, all of the detector charts are. Detectors are "normalized" to 662 keV.This implies that whatever it reads at Cs-137 is correct, and whatever it reads at any other energy needs to be compensated.Meters and MCA's do not compensate for this factor.
 
The response to equal numbers of photons of different energies is different. Far different tin fact. The same thing applies to a meter unit with a dial on it. Geiger Muller tubes do the same thing, with even more wiggles in the curve due to gas factors.
 
The reason I beat on this is that it is a fundamental principle, against which all our measurements are eventually made.
 
If this is not clear to all members, I will rethink how to explain it. It's that important.
 
Geo
 
 

#161 From: "Geo>K0FF" <GEOelectronics@...>
Date: Fri May 9, 2008 7:59 pm
Subject: ST-350 improvements
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Spectrum Techniques ST-350 is a self contained Geiger Muller Scaler-Counter Lab.
 
A built in digital counter, Ratemeter, Variable High Voltage Power Supply, Alarms,  and precision Programmable Timer makes the instrument a real joy for any kind of experiments using GM tubes.
 
Designed specifically for GM tubes, the input sensitivity is factory fixed at about 1.5 Volts. Naturally this is far to high for use with a scintillator probe.
Another handicap is the lack of a "clicker" to indicates counts being received. In a classroom environment, this is a must-have.
 
To their credit, Spectrum Techniques also recognized the value of both of those features, and have recently added them to their latest offering the ST-360, an updated version of the ST-350.
 
 
For those of us lucky enough to have the earlier version, all is not lost.
 
 My scintillator preamp project increases input sensitivity to 30 mV, perfect for scintillators,
 
and my Speak2Me module provides audio clicks.
 
 
 
A connection via the existing DB-9 connector on the back hooks the Speak2Me to the circuitry and in turn it provides the audio. Both the audio and preamp modules are self contained battery powered so there is no drilling or soldering required to add these features.
 
Schematics of both the Preamp and Speak2Me are located in FILES section of
 
Have fun
 
Geo
 
 

#160 From: "Geo>K0FF" <GEOelectronics@...>
Date: Thu May 1, 2008 2:34 pm
Subject: Projecto-dose
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Shine a small LED flashlight into the charger port of your CDV pen dosimeter and point the other end towards a wall or piece of white paper. The dosimeter scale will project out onto the target. It's backwards, but looks cool.
 
 
Have fun
 
Geo

#159 From: "Geo>K0FF" <GEOelectronics@...>
Date: Sun Apr 27, 2008 6:58 pm
Subject: ScintiLENi- The Ultimate FrankenGeiger?
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Finally, after all these years, one box has all the hacks in one place for the first time. Everything in this LENi was laid out some years ago as individual goals and the projects eventually came along one at a time.
 
Alpha-Beta-Gamma-X-Ray detection
 
Gamma Scintillator probe
Pancake Probe with Beta Shield
Count LED
Power on/Battery condition LED
Meter reset/zero push button.
Meter fast/slow toggle switch.
Speaker with Volume Control
Data Jack
Range X2 Multiplier switch
Rugged all metal meter
Rubber boots on switches
Sleek handle

Did I miss anything?

Oh yeah, it floats.
 
Have fun
 
Geo


#158 From: "Geo>K0FF" <GEOelectronics@...>
Date: Fri Apr 25, 2008 4:06 pm
Subject: Some Background on Background.
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NORM maps of interest

 
 
 
 
 
 
In NE MO where I live and have the Home Lab, background radiation runs around 10 uR/H from natural sources, mostly K-40. This radiation field will give far different counts on various probes, depending on their overall sensitivity and their sensitivity to the specific energies in the local radiation. For example K-40 has a radiation energy of 1460 keV, which is just above the normal range for GM tubes, therefore a GM tube will not give a totally accurate reading if K-40 is the main isotope. On the other hand, the low energies given off by U will be exaggerated by a good GM probe. On average though, GM tubes give very acceptable and particularly repeatable results.
 
By far the most common radioactive materials are the ones found in the soil
and rocks in most
every state of the Union in one form or another, and to a more or less
degree.

Almost all of the many isotopes represented in this group, are the decay
products or daughters of U235, U238 or Th-232. These include all the Radium's, Thorium's, Radon's, Polonium, all the way
down to the radioactive Leads. They all start out as one of the 3 parents
listed above, and here are a few excellent links that we continually refer to which give all the details.
 
See:
(click on link to download)
 
On this link print out at least item pages# 115,137,143,145 and 149
http://www.ocrwm.doe.gov/pm/program_docs/curriculum/unit_2_toc/50.pdf


and once again a link to the entire table of Nuclides:
http://atom.kaeri.re.kr/ton/nuc11.html
 
Background (B/G) is gamma rays, they travel far in air. Betas
do travel a distance too though and
shouldn't be overlooked, but are easily shielded out. Figure
12 feet per MeV in air for betas. Alphas not a problem,
only travel an inch or two in air.

Technically speaking, no amount of shielding will
*stop* gamma rays. Practically speaking, we refer to
Half Value Layer HVL, the amount that cuts it in half. Then you figure the
Tenth Value Layer or TVL as the most that can be achieved under
practical terms. The TVL depends on the energy of the
gammas, but 2" is TVL for a 1.5 MeV gamma. You can't have a 2 inch lead
shield in a handheld probe, so they are usually anywhere from 1/8" to
1/2" of lead.

In nature there are 3 decay chains headed by Uranium 235, Uranium 238 and
Thorium. U 235 in low abundance but U 238 and Thorium are everywhere. Each
of the decay chains have the long lived parent element and many shorter
lived daughters present in a stable mix called equilibrium. Sometimes
equilibrium is disturbed by natural means, but usually undisturbed ore has a
good mix. Keeping in mind that all U238 ores will have a similar  "signature",
be it yellow cake or Torbernite, because it is all Uranium after all. Many
different types of U samples are not needed, but interesting nonetheless.

Other radioactive isotopes also exist in nature but do not have a decay
chain, that is, their decay products themselves are not radioactive, but
stable. Potassium is a very common element, and a portion of all K in nature
is radioactive K-40, which is a large part of natural background radiation.
For home lab use, we can get samples of K-40 in N0-Salt, Potassium Chloride
salt for water softeners, fertilizer and many other household items.
The USGS has some cool maps that show distribution of radon
throughout the US as well as similar maps showing background Gamma
radiation. See:
http://energy.cr.usgs.gov/radon/radonhome.html
and
http://energy.cr.usgs.gov/radon/rnus.html
 
One of the first questions we hear on this board from a new member is "How hot
is this if I get a reading of XXX?).
Well, the answer depends on a lot of factors, namely the distance you are from
the radiation source, the size and shape of the radiation source, what is
between you and the source (including the source itself, can have large
self-absorption), and most importantly, what is the source material Quality
Factor "QF" ( i.e. what type, energy, and abundance of radiations does it
emit?)

In the field, one seldom encounters a single source of radiation, rather a
mixture of NORM ( naturally occurring radioactive material) which has an array
of different Gamma energies. Chief among the NORM are Uranium, Thorium and K-40.
A portion of all background (B/G) radiation detected will be from Cosmic Rays.
I've seen references that claim as much as 1/3 of all B/G is from Cosmic Rays,
although I personally cannot corroborate this. ( My experiments on bodies of
water yield very low residual counts, being well away from soil/rock and
soil/rock spawned radon).

From the lab standpoint, where shields can remove most of the B/G, individual
isotopes may be measured and formulae employed to ascertain the needed data.

One formula, taken from the Health Physics Handbook is shown here:

R (@1 ft)= 6 x CE
Or
R (@ 1 cm)= 5.6 x10^3 x CE

Where
R= RADs/H
C= activity in Curies
E= Gamma energy in MEV
x= multiplication symbol

Fortunately for us, the US Gov't has worked all this out for some useful
isotope, and an excerpt is included below. For a full read and printout , refer
to the source document at:
http://www-rsicc.ornl.gov

Here the "inverse square law" applies, so halving the distance will X4 the
intensity.












Exposure Rate Constants
The "Specific Exposure Rate Constant", sometimes known as the "Gamma Factor", is
the exposure rate at a specific distance from a given amount of a
photon-emitting radionuclide. These constants are used frequently for radiation
protection purposes. The following is a listing of Specific Exposure Rate
Constants for a variety of radionuclides, in units of Roentgens per hour (R/hr)
at a distance of one (1) meter from a one (1) curie point source of that
radionuclide.
Actinium
Ac-225 - 0.191364
Ac-227 - 0.0087468
Ac-228 - 0.84397
Aluminum
Al-26 - 1.49739
Al-28 - 0.88208
Americium
Am-241 - 0.313723
Am-242 - 0.202612
Am-242m - 0.18315
Am-243 - 0.312872
Am-244 - 1.17216
Am-245 - 0.086617
Am-246 - 0.079513
Antimony
Sb-117 - 0.304103
Sb-122 - 0.304251
Sb-124 - 1.06671
Sb-125 - 0.38036
Sb-126 - 1.7982
Sb-126m - 1.04488
Sb-127 - 0.444
Sb-129 - 0.85655
Argon
Ar-41 - 0.69597
Arsenic
As-72 - 1.16476
As-73 - 0.140008
As-74 - 0.54464
As-76 - 0.274096
As-77 - 0.0062863
Astatine
At-211 - 0.22644
At-217 - 0.000160247
Barium
Ba-131 - 0.46028
Ba-133 - 0.45547
Ba-133m - 0.124764
Ba-135m - 0.110038
Ba-137m - 0.39997
Ba-139 - 0.0285529
Ba-140 - 0.164502
Ba-141 - 0.57794
Ba-142 - 0.56869
Berkelium
Bk-250 - 0.67858
Beryllium
Be-7 - 0.0343804
Bismuth
Bi-206 - 2.5234
Bi-207 - 1.33311
Bi-208 - 1.5207
Bi-211 - 0.047138
Bi-212 - 0.194768
Bi-213 - 0.11618
Bi-214 - 0.83916
Bromine
Br-77 - 0.71151
Br-80 - 0.080142
Br-80m - 0.703
Br-82 - 1.61949
Br-83 - 0.0051837
Br-84 - 0.88504
Br-85 - 0.039183
Cadmium
Cd-109 - 0.184371
Cd-111m - 0.313131
Cd-115 - 1505160000
Cd-115m - 0.0127021
Cd-117 - 0.6438
Cd-117m - 1.08595
Calcium
Ca-45 - 2.98664E-08
Ca-47 - 0.58497
Ca-49 - 1.33755
Californium
Cf-248 - 0.045473
Cf-249 - 0.41403
Cf-250 - 0.044844
Cf-251 - 0.42994
Cf-252 - 0.041847
Cf-253 - 0.0007696
Cf-254 - 4.8507E-08
Carbon
C-11 - 0.71669
Cerium
Ce-139 - 0.205498
Ce-141 - 0.073223
Ce-143 - 0.255041
Ce-144 - 0.0233174
Cesium
Cs-126 - 0.80142
Cs-129 - 0.359825
Cs-131 - 0.124431
Cs-132 - 0.57572
Cs-134 - 0.99937
Cs-134m - 0.070448
Cs-136 - 1.34384
Cs-137 - 0.38184
Cs-138 - 1.26614
Cs-139 - 0.15762
Chlorine
Cl-38 - 0.71854
Chromium
Cr-49 - 0.75073
Cr-51 - 0.023384
Cobalt
Co-56 - 1.92585
Co-57 - 0.151219
Co-58 - 0.61383
Co-58m - 9.7569E-05
Co-60 - 1.37011
Co-60m - 0.00335109
Co-61 - 0.084582
Copper
Cu-61 - 0.56832
Cu-62 - 0.7067
Cu-64 - 0.131942
Cu-67 - 0.087431
Curium
Cm-242 - 0.072113
Cm-243 - 0.47582
Cm-244 - 0.064417
Cm-245 - 0.4514
Cm-246 - 0.057387
Cm-247 - 0.267029
Cm-248 - 0.045399
Cm-249 - 0.0148259
Dysprosium
Dy-157 - 0.309209
Dy-165 - 0.0229141
Dy-166 - 0.05735
Einsteinium
Es-253 - 0.0256077
Es-254 - 0.5513
Es-254m - 0.56203
Es-255 - 0.00315573
Erbium
Er-169 - 1.26022E-06
Er-171 - 0.29637
Europium
Eu-152 - 0.74444
Eu-152m - 0.212602
Eu-154 - 0.75554
Eu-155 - 0.066748
Eu-156 - 0.73704
Fermium
Fm-254 - 0.041477
Fm-255 - 0.322677
Fluorine
F-18 - 0.69523
Francium
Fr-221 - 0.044141
Fr-223 - 0.33041
Gadolinium
Gd-153 - 0.172383
Gd-159 - 0.039183
Gd-162 - 0.308617
Gallium
Ga-66 - 1.29648
Ga-67 - 0.111148
Ga-68 - 0.66193
Ga-72 - 1.45632
Germanium
Ge-68 - 0.060458
Ge-71 - 0.061161
Ge-77 - 0.71558
Gold
Au-194 - 0.66008
Au-195 - 0.087394
Au-195m - 0.152884
Au-196 - 0.369704
Au-198 - 0.291634
Au-199 - 0.069042
Hafnium
Hf-181 - 0.39257
Holmium
Ho-166 - 0.023199
Ho-166m - 1.0619
Indium
In-111 - 0.50172
In-113m - 0.242979
In-114 - 0.0230251
In-114m - 0.150738
In-115m - 0.197173
In-116m - 1.3542
In-117 - 0.50283
In-117m - 0.11322
Iodine
I-122 - 0.70337
I-123 - 0.276686
I-124 - 0.7585
I-125 - 0.274984
I-126 - 0.39035
I-128 - 0.059792
I-129 - 0.125837
I-130 - 1.40267
I-131 - 0.282939
I-132 - 1.42746
I-133 - 0.40885
I-134 - 1.57287
I-135 - 0.86099
I-136 - 1.26429
Iridium
Ir-190 - 0.99197
Ir-190m(1.2h) - 2.2644E-07
Ir-190m(3.2h) - 0.055463
Ir-192 - 0.59163
Ir-193m - 0.00037629
Ir-194 - 0.061901
Ir-194m - 1.61764
Iron
Fe-52 - 0.52281
Fe-59 - 0.66193
Krypton
Kr-79 - 0.60347
Kr-81 - 0.43364
Kr-83m - 0.118733
Kr-85 - 0.00156584
Kr-85m - 0.160136
Kr-87 - 0.43253
Kr-88 - 1.02453
Kr-89 - 0.97162
Kr-90 - 0.76701
Lanthanum
La-141 - 0.0226144
La-142 - 1.35272
Lead
Pb-203 - 0.67636
Pb-204m - 1.3505
Pb-205 - 0.251193
Pb-210 - 0.251637
Pb-211 - 0.0363932
Pb-212 - 0.273393
Pb-214 - 0.323454
Pd-103 - 0.230103
Pd-109 - 0.0004847
Lutetium
Lu-177 - 0.0282532
Lu-177m - 0.78144
Magnesium
Mg-27 - 0.53613
Mg-28 - 0.87875
Manganese
Mn-52 - 2.0091
Mn-52m - 1.44411
Mn-54 - 0.51134
Mn-56 - 0.92352
Mn-57 - 0.112147
Mercury
Hg-197 - 0.069338
Hg-197m - 0.076183
Hg-203 - 0.253117
Molybdenum
Mo-101 - 0.88467
Mo-91 - 0.70226
Mo-93 - 0.293632
Mo-99 - 0.112924
Neodynium
Nd-147 - 0.139453
Nd-149 - 0.300144
Neptunium
Np-235 - 0.258223
Np-236 - 1.04821
Np-236m - 0.23643
Np-237 - 0.46287
Np-238 - 0.55389
Np-239 - 0.51282
Np-240 - 1.41562
Np-240m - 0.42328
Nickel
Ni-56 - 1.08817
Ni-57 - 1.07707
Ni-65 - 0.297406
Niobium
Nb-90 - 2.44089
Nb-91 - 0.326784
Nb-91m - 0.26492
Nb-92 - 1.26318
Nb-92m - 0.89281
Nb-93m - 0.052577
Nb-94 - 0.97976
Nb-94m - 0.202797
Nb-95 - 0.48026
Nb-95m - 0.23643
Nb-96 - 1.5244
Nb-97 - 0.43475
Nb-97m - 0.46694
Nitrogen
N-13 - 0.71706
N-16 - 1.47408
Osmium
Os-185 - 0.4847
Os-190m - 1.11666
Os-191 - 0.067969
Os-191m - 0.0053613
Os-193 - 0.052318
Oxygen
O-15 - 0.7178
Platinum
Pt-191 - 0.243756
Pt-193m - 0.0172013
Pt-195m - 0.075073
Pt-197 - 0.0208939
Pt-197m - 0.071447
Plutonium
Pu-236 - 0.088985
Pu-237 - 0.38443
Pu-238 - 0.078995
Pu-239 - 0.0301365
Pu-240 - 0.07511
Pu-242 - 0.062308
Pu-243 - 0.092833
Pu-244 - 0.054094
Pu-245 - 0.38702
Polonium
Po-209 - 0.00363007
Po-210 - 5.2688E-06
Po-211 - 0.0049136
Po-213 - 1.90402E-05
Po-214 - 5.1726E-05
Po-215 - 0.000105857
Po-216 - 8.9688E-06
Potassium
K-40 - 0.081696
K-42 - 0.143153
K-43 - 0.67007
Praseodynium
Pr-142 - 0.0299922
Pr-143 - 5.6388E-09
Pr-144 - 0.01702
Pr-144m - 0.0367521
Promethium
Pm-143 - 0.266992
Pm-144 - 1.09446
Pm-145 - 0.089466
Pm-146 - 0.54094
Pm-147 - 2.67584E-06
Pm-148 - 0.330669
Pm-148m - 1.31979
Pm-149 - 0.0085729
Pm-151 - 0.262182
Protactinium
Pa-230 - 0.88319
Pa-231 - 0.37407
Pa-233 - 0.49395
Pa-234 - 1.98172
Pa-234m - 0.0102712
Radium
Ra-222 - 0.0078255
Ra-223 - 0.325193
Ra-224 - 0.0109779
Ra-225 - 0.154068
Ra-226 - 0.0121138
Radon
Rn-218 - 0.00050579
Rn-219 - 0.052503
Rn-220 - 0.000359751
Rn-222 - 0.00027343
Rhenium
Re-182 - 1.13886
Re-182m - 0.73778
Re-183 - 0.157509
Re-184 - 0.58201
Re-184m - 0.284086
Re-186 - 0.0181633
Re-188 - 0.040478
Rhodium
Rh-103m - 0.0255744
Rh-105 - 0.058756
Rh-105m - 0.157287
Rh-106 - 0.138158
Rubidium
Rb-81 - 0.83768
Rb-82 - 0.77848
Rb-83 - 0.77145
Rb-84 - 0.86062
Rb-86 - 0.053946
Rb-88 - 0.321937
Rb-89 - 1.0952
Rb-90 - 0.94276
Rb-90m - 1.63873
Ruthenium
Ru-103 - 0.33189
Ru-105 - 0.51689
Ru-97 - 0.44178
Samarium
Sm-151 - 9.0354E-05
Sm-153 - 0.09028
Scandium
Sc-44 - 1.33274
Sc-46 - 1.16735
Sc-46m - 0.066933
Sc-47 - 0.08029
Sc-48 - 1.89329
Sc-49 - 0.00052059
Selenium
Se-73 - 1.09853
Se-75 - 0.85951
Silicon
Si-31 - 0.00048322
Silver
Ag-106m - 1.93769
Ag-108 - 0.0162763
Ag-108m - 1.27132
Ag-109m - 0.100714
Ag-110 - 0.0205646
Ag-110m - 1.65242
Ag-111 - 0.0197173
Sodium
Na-22 - 1.3394
Na-24 - 1.93769
Strontium
Sr-82 - 0.39405
Sr-85 - 0.75924
Sr-85m - 0.222148
Sr-87m - 0.29637
Sr-89 - 8.1585E-05
Sr-91 - 0.41366
Sr-92 - 0.72002
Sr-93 - 1.35605
Tantalum
Ta-182 - 0.77182
Technetium
Tc-101 - 0.255892
Tc-95 - 0.77404
Tc-95m - 0.71743
Tc-96 - 1.81263
Tc-96m - 0.16391
Tc-97 - 0.281052
Tc-97m - 0.193621
Tc-98 - 0.8991
Tc-99 - 4.5954E-07
Tc-99m - 0.122729
Tellurium
Te-121 - 0.53835
Te-121m - 0.248011
Te-123 - 0.099419
Te-123m - 0.194657
Te-125m - 0.228216
Te-127 - 0.00348836
Te-127m - 0.073149
Te-129 - 0.067821
Te-129m - 0.073889
Te-131 - 0.298775
Te-131m - 0.90724
Te-132 - 0.279313
Te-133 - 0.58608
Te-133m - 1.36493
Te-134 - 0.64047
Terbium
Tb-157 - 0.0089762
Tb-160 - 0.66156
Tb-162 - 0.71188
Thorium
Th-226 - 0.067266
Th-227 - 0.42365
Th-228 - 0.079254
Th-229 - 0.73593
Th-230 - 0.068857
Th-231 - 0.54501
Th-232 - 0.068376
Th-233 - 0.095719
Th-234 - 0.075406
Thullium
Tm-170 - 0.0061901
Tm-171 - 0.00096089
Tin
Sn-113 - 0.179228
Sn-117m - 0.251452
Sn-119m - 0.103193
Sn-123 - 0.0039294
Sn-125 - 0.172938
Sn-126 - 0.126096
Titanium
Ti-200 - 0.83361
Ti-201 - 0.087764
Ti-202 - 0.349206
Ti-204 - 0.00111518
Ti-207 - 0.00130388
Ti-208 - 1.70385
Ti-209 - 1.29352
Ti-210 - 1.70237
Ti-44 - 0.144633
Ti-45 - 0.61161
Ti-51 - 0.26381
Tungsten
W-181 - 0.051393
W-185 - 2.02205E-05
W-187 - 0.328782
W-188 - 0.00133755
Uranium
U-230 - 0.091131
U-231 - 0.7844
U-232 - 0.088911
U-233 - 0.0291042
U-234 - 0.077589
U-235 - 0.338883
U-236 - 0.073704
U-237 - 0.58793
U-238 - 0.065231
U-239 - 0.13431
U-240 - 0.284382
Vanadium
V-48 - 1.70126
V-52 - 0.76109
Xenon
Xe-122 - 0.180079
Xe-123 - 0.52392
Xe-125 - 0.356014
Xe-127 - 0.345247
Xe-129m - 0.228105
Xe-131m - 0.093721
Xe-133 - 0.102971
Xe-133m - 0.112258
Xe-135 - 0.189477
Xe-135m - 0.320087
Xe-137 - 0.123802
Xe-138 - 0.62123
Ytterbium
Yb-169 - 0.326969
Yb-175 - 0.0304621
Yttrium
Y-86 - 2.32804
Y-87 - 0.68857
Y-88 - 1.78303
Y-90m - 0.48692
Y-91 - 0.00199911
Y-91m - 0.38036
Y-92 - 0.146927
Y-93 - 0.051652
Zinc
Zn-62 - 0.33263
Zn-65 - 0.330188
Zn-69 - 4.3216E-06
Zn-69m - 0.295371
Zirconium
Zr-86 - 0.88171
Zr-88 - 0.6327
Zr-89 - 0.98494
Zr-95 - 0.46546
Zr-97 - 0.108114
**Listing partially extracted from ORNL/RSIC-45, "Specific Gamma-Ray Dose
Constants for
Nuclides Important to Dosimetry and Radiological Assessment", 1981
 
Taking a Radiation Reading" is a simple matter. Understanding that
reading may be a little more complex. Yes you can point your CDV700
at something, and get a reading. The next question is "what does that
reading mean?".

The passage that follows is a direct quote from a book, so that the
details are preserved. My comments at the conclusion.

QUOTE:
"To be effective in your radiological work, you must get a first
grasp on the ways radiation is measured. "Radiation", like "distance"
is a general concept. You would have a weak understanding of distance
if you were vague about "foot", "inch", "mile", "kilometer", "light
year", and the other ways by which distance is measured. The same is
true for radiation.


The Curie (Ci) is the unit used to measure the activity of all
radioactive substances. It is a measurement of rate of decay or
nuclear disintegration that occurs within the radioactive material.
The Curie initially established the activity ( that is, decay rate)
of Radium as the standard with which the activity of any other
substance was compared.

By using a formula that takes into account the number of atoms per
gram and the value of the half-life in seconds, scientists have
determined that the activity of Radium is equal to 3.7 X 10E10
nuclear disintegrations per gram per second. This value is now the
standard of comparison. A Curie of ANY radioactive isotope,
therefore, is the amount of that isotope that will produce 3.7 X
10E10 nuclear disintegrations per second. Since the measure is based
on number of disintegrations, the weight of the radioisotope will
vary from that of Radium. A Curie of pure CO60 would weigh less
than .9 milligrams, while a Curie of U238 would weigh over two metric
tons.

The Curie is a large unit. In training, a milliCurie, mCi (one-
thousandth Curie) and the microCurie, uCi ( one millionth Curie) are
common units in use. At the opposite extreme, the Curie is too small
a unit for convenient measurement of the high-order activity produced
by the nuclear explosion. For this purpose, he MegaCurie ( one
million Curies) is used.

The Roentgen,(R) by definition measures exposure to Gamma and X-rays.
It is an expression of the ability of Gamma or X-ray to ionize air.
One R will produce 2.083 X 10E9 ion pairs per cubic centimeter in
air.

The Curie measures Radioactivity
The Roentgen measures X or Gamma rays"
END QUOTE

My comment:
Armed with the above information, consider the added confusion when
you include the fact that every radioisotope puts out a different
type of radiation mixture. Some have Alphas and Betas(Betas
themselves which have a range, not a discrete energy). Then the Gamma
rays are of different energies. This soup of different radiations
would be difficult enough to quantify in a perfect world, but our
probes are far from perfect. Some respond way differently than
others, some over respond to certain radiation, or under respond. The
probe housing also has a big affect on the final readings..........
some being "compensated", some "uncompensated. Throw in the distance,
geometry and other geotropic factors, shielding, and it would be very
difficult indeed to say "this material is 20 mCi" First you would
have to know exactly what the material was in the first place, so you
could analyze which radiations the probe was ( or was not) reading.



Since the R is a unit of field charge and not of radioactivity, it is
perfectly valid to use a CDV700 to make these measurements ( shield
closed). It is also valid to use a Beta check source to "calibrate" a
probe/meter combination and have that "calibration" apply to the
Gamma response as well*. That reading is valid for the location of
the probe. It offers no help as to the quantity or energy level of
the material producing the Gamma Rays, or the distance it is from the
probe. It does not matter in this context, the ionization field is
being produced by whatever quantity and energy mix that exists, and
the distance factor is automatically integrated into the reading. R
is a measure of the effects of Gamma rays, only valid with the Beta
shield close.
That's fine from a health-physics or CD standpoint, as far as it
goes.

* the idea here is that the characteristics of the QPL 6993 probe are
so well known, both Beta and Gamma, that exposure to a know Beta
source ( shield open) will give a reasonable expectation of a know
Gamma response ( shield close). This is the basis of the QPL or
Quality Product List classification on the 6993 tubes. In the case of
the radioactive check source that comes with the CDV700 set, there
has been a considerable time elapse since these were installed, and
in some cases at least, they have been replaced or refreshed. Also it
is indicated that the material itself is of different compositions,
between makers. All this affects the present day strength of he
sample. Since we have a "standard" radioactive source readily
available, long half-life, namely the radioactive lantern mantles,
assuming them to be from the same batch lot ( mine are), it would
seem that anyone could measure his probe/meter against the mantle,
then apply a K factor to the onboard test spot. All we would need is
a representative measurement made with a new or know good tube at the
specified high voltage. A suggestion is to leave the mantle in the
plastic bag, with the red side towards the probe, and wrapped around
the open Beta window with a rubber band. Perhaps someone out there
has an actual assayed or calibrated lab sample that could provide the
NIST trace to legitimize the project.



My personal interest goes in another vector. I want to know
quantitatively ( assay) and qualitatively ( is it Alpha?, Beta?,
Gamma?, and what energy levels). I continue to give reading as CPM,
with probe and other conditions listed.

Geologists have a keen interest in radioactivity, as it can foretell
the
nature of the earth in the vicinity. Some even use the small
differences to
detect the probable presence of petroleum. Others use it to prospect
for
minerals.

In practice the 3 main of interest are Potassium, Uranium and
Thorium. By knowing the concentration and relationship of these three, the
geologist can make many conclusions.

A small percentage ( .12%)of all natural Potassium is a radioactive
isotope
K-40 which has only one Gamma decay product, a ray of 1.461 MeV. This
can be
measured directly by the instrument.

Uranium itself is an strong Alpha emitter and it's gamma rays are
unsuitable
for direct measurement in this field, so a daughter of unique
properties,
Bismuth-214 is used instead, where the 1.76 MeV Gamma can easily be
distinguished.

Thorium has similar difficulties in direct measurement, so in this
instance
the daughter - Thallium-208 with it's 2.62 MeV gamma are chosen for
scrutiny.

We you see prospectors with their PRI's clicking away in the movies,
the
real science of today has moved way beyond that. Grids are set up for
a
routine survey and many measurements of the 3 minerals mentioned
above are
made. Sometimes the detector is winched down a well drill hole to take
measurements ( other methods of radioactive investigation are also
used in
well logging). Airborne and carborne surveys can easily be made too.

In all these cases, the 3 different energy level gammas are measured
separately by means of a gamma spectrometer. Some instruments are more
complex than others, thereby giving readings that are easier to
understand.
Some even use isotope stabilized probes to prevent temperature
variations
form affecting readings ( NaI(Tl) - PMT scintillators sensitivity
drifts
with temperature, about 1% for each 2 degrees). A closed feedback loop
measures the Alphas given off by Am-241 which is actually inside the
crystal, and the high voltage is adjusted for a standard reading
automatically.

As you should know if you read the Primer in GCE message 266, scintillator
detectors put out pulses that vary in height, according to the energy
level
of the radiation that caused the pulse. In the Gamma Ray
Spectrometer, those pulses are sorted out and dealt with on a case by case basis.
 In the simple self-contained ( probe is inside the instrument) units like the DISA
300, there is often only a LLD ( Lower Level Discriminator) sometimes
called a threshold control. It can be preset for the different channels of
interest, but basically it will ignore all the energy pulses BELOW a certain
point, and count all the ones above that. The K channel ( Potassium) will
ignore all below 1.46 but count all above that, which of course includes the
U and Th channels. Similarly the U ( Uranium) channel will include the Th
energies., so to get an individual picture of each, some readings are
taken, and mathematical subtraction employed.

In the case of the more complicated Scintrex, there is also a Upper
Limit control or "window" applied which ignores all the pulses ABOVE a
certain level, so that the counter only recognizes the pulses above the LLD
but below the Window.

These same controls exist on all SCA's ( Single Channel Analyzers)
except that in the geologists special unit there a 4 different ones that are
simply preset, then switch selected ( K-U-Th and the 4th channel is wide
open or Total Counts).

Rather large scintillators must be utilized for good sensitivity and reasonable count
rates. Even though the count rate "wide open" will be huge, when all the
random pulses are screened out, the actual reading can become quite small
for the energy levels of interest.
 
Have fun
 
Geo


 

#157 From: "Geo>K0FF" <GEOelectronics@...>
Date: Fri Apr 18, 2008 5:49 pm
Subject: Fw: Midwest Earthquake-NORM radiation changes?
k0ff
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----- Original Message -----
From: Geo>K0FF
Sent: Friday, April 18, 2008 12:18 PM
Subject: Midwest Earthquake-NORM radiation changes?

 

It would be interesting to note if today's rather rare earthquake in the Wabash Fault has in any way changed the normal
background radiation in the Midwest area. Anyone in that region have a 24/7 monitor running?
 
George Dowell
New London Nucleonics Lab
 

#150 From: "Geo>K0FF" <GEOelectronics@...>
Date: Tue Apr 8, 2008 3:24 pm
Subject: Advanced Experiments in Physics
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#149 From: "Geo>K0FF" <GEOelectronics@...>
Date: Wed Mar 26, 2008 11:19 pm
Subject: Nuclear Fission in the Home Radiation Lab
k0ff
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Nuclear Fission in the Home Radiation Lab
 

SF, Spontaneous Fission is a form of radioactive decay that
is possible in very heavy atoms. Theoretically it can happen in all atoms above A=100, but in practice SF is only probable in atoms above A=230.
 
Elements U-235 (2.0 E10-7%), U-238 (5.4 E10-5%), Pu-239 (4.4x10-10 %), Pu-240 (5.0x10-6 %) and Cf-252 (3.09 %) are all candidates for SF, with Cf-252 far and away the most prodigious with fission probability of 3.09% per decay.
 
Neutron "background" baseline established over several days of monitoring with the Fast Neutron Bubble Detector.
At our altitude of 600 Ft., temperature of 73 F and 48 hours, no bubbles were noted.  Geology in this region, ne Missouri USA,  is limestone, from the sediment of the ancient inland sea.
 
SF Source is a Depleted Uranium collimator weighing 1 pound 12 ounces, the detector being a BTI BD-PND bubble detector.
Calculated neutron yield for this mass is 11 n/s.

 

At a distance of 2.5 cm, bubs are running 4 or 5 per day.
 
 
 
 
INDUCED FISSION in the HOME RAD LAB
Subcritical Neutron Multiplication
 
Described is a lab procedure for splitting of U-235 atoms and recording the results in terms of fast neutrons
via BTI Bubble Detector Model BD PND. By experiment we have verified that the BD PND only responds to fast neutrons, nit slow neutrons, and also that there are zero "background" neutrons at this location. Spontaneous fission from the DU slab has been documented and is subtracted from the overall results, although the number of SF neutrons is quite small.
Fast initiator neutrons are provided by a home made Ra-Be generator, constructed for the project from 10,000 Radium
watch hands plus elemental Beryllium. Yield was about 240 CPM into a moderated and reflectored 20 atm.He3 detector.This source was temporary and has since been dismantled.
 
Fast neutrons are first thermalized ( slowed down) by layers of high density polyethylene plastic, called HDPE from here on, a hydrogen rich material.
A beam of slowed neutrons is presented to a DU metal slab (note 1) consisting of approximately 1.75 pounds of U-238 and about 1.2 grams of U-235.
When a neutron is absorbed by a U-235 atom, the atom becomes unstable U-236 and immediately fissions via one of several methods shown below. Each of the methods results in the release of either 2 or 3 fast neutrons, therefore we use the average figure of 2.5 released neutrons in the formula.
We have now multiplied the original fast neutron from the Ra-Be source to 2.5 neutrons. By judicious use of HDPE moderators and graphite reflector slabs, the extra
neutrons are slowed and reflected back to be themselves presented top the DU target. These new neutrons continue the subcritical multiplication process.
 
Ra+Be= 1n (fast)
 
Fast n + HDPE= 1n (thermal)
 
Thermal n + U-235 = U-236 = Kr-92+Ba-141 (note 2)+ 2.5 n (average, Fast)
 
2.5 Fast n + HDPE+C (reflector) = 2.5 n (slow)
 
2.5 Thermal n + U-235...etc.etc.= many n (fast) for detection via BTI Bubble detector.
 
 
 
Regular U metal (non-DU) impossible to find today. DU easy to find, various forms. DU contains about .2% U-235.
 
HDPE is 6" x 6" x .5" slabs so is the graphite. Making adjustable piles and taking measurements eventually yields a standard configuration. Neutron generator was 10,000 radium watch hands + Be. 
 
Only a bubble detector can be used in this scheme because of long count times, and the absolute zero false bubbs.

Bubbles captured from exposure to the DU target while it was being bombarded with slow neutrons.

 

Bubble detector test using only the slowed neutrons, without the DU slab shows 5 or 6 small bubbles
during a similar measured time period.
Note that the two larger bubbles in this picture were there before the test was run and must be disregarded.

Above is a test showing fast neutrons captured right next to the bare source, that is no

modereator. There were 8 bubbles left in the BTI from previous tests, and they should be

disregarded in the total count here. These include those two large bubbles.

 
Bubble detector test without any source, without ant DU, yields no bubbles ( zero background).
 
 
 
note 1- USA laws and rules allow for up to 15 pounds of DU metal without a license, nor
is there any restriction on the number of Radium Watch hands that can be owned.
note 2:
other possible fission products-
U-235 + n = Ba-144 + Kr-90 + 2n + energy
 
U-235 + n = Ba-141 + Kr-92 + 3n + 170 MeV
 
U-235 + n = Zr-94 + Te-139 + 3n + 197 MeV
 
Have Fun

George Dowell, “Geo”

NLNL/ New London Nucleonics Laboratory

Copyright © Viscom Inc. 2007

The treatise may under no circumstances be resold or redistributed in either printed, electronic,

or any other forms, without prior written permission from the author.

Comments, criticism and questions will be appreciated and may be directed to

the author by email to GEOelectronics@netscape.com                                   

                                                                                                                                       

All PHOTOS © by the author unless noted otherwise

 
 
 

#147 From: "Kevin" <vk3ukf@...>
Date: Fri Mar 14, 2008 11:47 am
Subject: A.A.E.C. field I.D. book.
vk3ukf
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Greetings group,

my name is Kevin,

I have had an interest in mineralogy for some time, and have found
an old friend I used to toke around with me years ago.

Something that might interest the mineralogist in you is a scan of a
field pocket manual I obtained from the Australian Atomic Energy
Commission (A.A.E.C.)in the mid seventies.

It is entitled Selected Uranium Mineral Specimens and is a pdf/zip
download.

http://www.vk3ukf.com/vk3ukf_files/eBook/SUMS.htm

I guess it's an eBook then.

There's probably some other stuff there, that some of you would get,
you'll have to look at the menu on the main page.

http://www.vk3ukf.com/index2.htm

All the best.
Kevin, VK3UKF.

#146 From: "Don Jordan" <DonJordan@...>
Date: Thu Feb 21, 2008 3:52 pm
Subject: Fw: [GeigerCounterEnthusiasts] Newbie needs pointing in the right direction.
dkjordan2001
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----- Original Message -----
Sent: 18 February, 2008 12:06 PM
Subject: Re: [GeigerCounterEnthusiasts] Newbie needs pointing in the right direction.

Don, nice summary. Please add the word "activity" to the Ci-specimen explanation, add neutron Q factor and
then post the article to

http://tech.groups.yahoo.com/group/HomeRadLab/

THANKS

Geo

--- DonJordan@ramservicesinc.com wrote:

From: "Don Jordan" <DonJordan@ramservicesinc.com>
To: <GeigerCounterEnthusiasts@yahoogroups.com>
Subject: Re: [GeigerCounterEnthusiasts] Newbie needs pointing in the right direction.
Date: Mon, 18 Feb 2008 11:58:48 -0600

Becquerels [Bq] and Curies [Ci] measure how much radioactive stuff you have while Rems and rads (as well as Sieverts) measure how much radiation damage is being done to living tissue. The rad measures how much ionization energy the radiation deposits in your body while the rem is intended to measure how damaging that energy may be:  rems = rads*Q

The Quality factor Q is 1 for beta, gamma, and X-rays.  The Q factor for neutrons varies from 2 to 11 for neutron radiation depending on the neutron energy.  Alpha radiation cannot penetrate into living tissue from outside the body, so its Q factor of 20 only applies to internally deposited alpha emitters.

Note that we do not measure amounts of radioactive material by weight (e.g., grams) because that doesn't tell you much directly.  Instead we use the ACTIVITY of the sample measured in Bq or Ci because this tells you directly how much radiation is coming from a given specimen and you can then directly calculate the radiation dose you would receive.

The "average" radiation exposure from background sources in the USA is about 350 millirem per year or about 1 millirem per day. Hope this helps.

----- Original Message -----
From: carpentershop
To: GeigerCounterEnthusiasts@yahoogroups.com
Sent: 15 February, 2008 10:48 PM
Subject: [GeigerCounterEnthusiasts] Newbie needs pointing in the right direction.

Hi guys,

I found this group from an Ebay seller a while back and finially
joined up a few days ago. Interesting group...

I am in the countertop business, granite, quartz, solid surface and
laminate, as well as kithens. The current controversy over granite
is what has motivated me to learn about Geiger counters and hopefully
be able to understand measuring radiation better.

I do have a few question that I would like the groups opinion on.

1. Has anyone done any testing on granite materials?

Some of the granites in studies show as much as 32 Bq per square
meter per day. I noticed that you guys talk in Rems and Rads, the
conversion gets my head spinning at times, no head for math at all.

2. Can anyone recomend a good Geiger counter for testing granite
materials that we offer the public?

I am not sure I buy the scare mongers, but some of the studies are
calling for the testing of granite and if they are concerned, I
figure I had better get ahead of the issue.

I've been reading the new posts, hadn't found the time to go back to
the old ones, but there seems to be a lot of talent here along with a
passion for the feild.

Thanks,
Al

__________________________________________________________
Netscape. Just the Net You Need.


#145 From: "carpentershop" <al@...>
Date: Mon Feb 18, 2008 12:18 am
Subject: Granite radiation files
carpentershop
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Hello,
Geo pointed me to this Yahoo group and mentioned there was some
previous work done on granite by this group.   I looked in the Files
section but did not see it.

Is this info still available?

Thanks,
Al

#144 From: "Geo>K0FF" <GEOelectronics@...>
Date: Sun Jan 20, 2008 7:16 pm
Subject: Sierra Madre Occidental field trip> Jan 2008
k0ff
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When rock collecting in Missouri turns from rock picks to ice picks, we search for easier prospecting grounds.
This January it was Puerto Vallarta, Jalisco, Mexico.
 
From Pto Vall, we journeyed by boat and then horseback to the Sierra Madre Occidental Mountains rain forest, where collecting was enjoyable and easy.
Members of our group were from Cuba, Venezuela, Canada and Germany.
 
The instrument of choice for radiation surveying was one of my PM1703M pocket scintillators.
 
Gamma studies were performed on the airplane from zero to 33,000 feet, on a metal boat in Pacific Ocean's Bahía de Banderas, on a fiberglass boat out in the Pacific, and of course on the ground in the rain forest. Members of out group came from Canada, Cuba, Germany, Russia and Venezuela.
 
Some very interesting radiation facts were observed and will be reported in full on the link site soon as I can get them all typed up.
 
Mainly we wanted to see how low we can get the background radiation to read out in the ocean, away from metal and rocks. With the normal background on the beach at 12 to 16 uR/H, the fiberglass boat was the lowest achievable at only 2 uR/H. We were far enough out to be completely out of range of background from rocks, and the readings were steady enough to indicate that the Radon and daughters in the wind were not much of a factor either, leaving radiation from our own bodies, and Cosmic Rays as the only significant source.
 
Speaking of Cosmic Rays, we did a Gamma Survey starting at the PVR airport on the ground at almost zero elevation  ( 8 uR/H) up to 33,000 feet ( 26 to 28 uR/H) and back down to about 500 feet at STL. Paying particular attention to the decent stage, from the peak of high 20's, one could observe the rate falling off steadily according to altitude, but not all the way down to ground level. At what I estimate to be 4000 to 5000 feet, the readings leveled off and failed to decline significantly from there to the ground at STL and 4 uR/H.
 
The conclusion is that at a certain altitude, there is already enough air above you to attenuate or convert most of the easily measured Cosmic rays. Later we envision a field trip to the top of Pikes Peak, loaded with more equipment to make even more measurements, including neutron survey vs. altitude.
 
At this time the link only has the raw photo log, but you may enjoy browsing it until the article is completed. 
 
Winter in Missouri
Deciding to go on field trip on New Year eve at local winery
whee.
Pier at PV
Leaving civilization
Whale watching
Porpoise watching
Shark watching
Diving break at the Los Arcos dive park
Arriving fishing village See note 3 on sign.
Iguanas everywhere
Hiking to horses
Locals wash clothes on these rocks in the river
Trailhead
Rain forest
Radiation Detector equipped horse
Rough trail up mountain
Waterfall and river
Radiation reading, granite boulders
Geo's horse drinking in river
Villages in rain forest
Back to the beach for a rest
View of palm tree through my hat during siesta on the beach
Back to PV, goofy hat.
Back to civilization at the PV marina
Shops in downtown PV
Mexican Navy Museum PV
Cosmic Ray study on jet
 
 
 
 
Anyone having ideas for similar field trips, send your suggestions and plane tickets to me.
 
Have fun
 
Geo
(Hor-hey)
 
 
 
 

#143 From: "Geo>K0FF" <GEOelectronics@...>
Date: Mon Jan 7, 2008 5:10 pm
Subject: Detecting DU at a distance via beta particle emission.
k0ff
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Detecting DU at a distance via beta particle emission.

 
DU (Depleted Uranium) is uranium with the majority of the U-235 removed, leaving behind U-238 and U-234.
I prefer to think of DU as refined U-238. The metal has many industrial and scientific uses, mainly because of its high density, being 1.7 times as dense as lead. A few using would be counterweights and radiation shielding. DU is used in projectiles because of its unique density, pyrophoricity and "self-sharpening" characteristics.
 
The only progeny present that can be detected at a distance would be Pa-234m, a beta emitter.
With a maximum energy of  2.28 MeV, the betas would travel approximately 20-25 feet in air, using the rule of thumb of 10-12 feet per MeV.
A sensor would have to be appreciably closer than the maximum distance to detect the beta particles.
 
Because of self-shielding, DU metal's surface beta rate is in ratio of the surface size, not the thickness or
volume of the sample. In other words a thin sheet would have the same beta surface emission rate as a thick sheet.
Indeed, DU Slabs are used in the lab to calibrate probes.
 
The best "calculations" are done in the lab with a DU slab and a detector! Using a 2 pound cylinder of DU metal and
a pancake probe, about 6 feet is as far as you can get and still obtain usable (statistically significant) readings. Any closer and the readings
ramp up quickly. With a 100 Cm^2 alpha-beta scintillator on a Thermo ELECTRA alpha-beta meter, the range is extended to about 10 to 12 feet.
 
Geo

#142 From: "Keith Watt RN" <kw@...>
Date: Sat Jan 5, 2008 4:28 pm
Subject: Quartz Fibre Dosimeters
keith_wattuk
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Hello, I have some Dosimeters that can be seen in the group's photos
section at;

http://tech.ph.groups.yahoo.com/group/HomeRadLab/photos/view/6a9c?b=1

I have lost 2 of my low dose Quartz Fibre Dosimeters and I am looking
to try and find low cost replacements for them. They are not used
professionally, so I'm not looking to pay professional prices.

The 2 Dosimeters in the photo have ranges 0 - 200 ROENTGENS, the
other is 0 - 150 r (which I assume is the same as 0 - 150 ROENTGENS).

The ones I lost were 0 - 0.2r, again I am guessing that's 0 - 200
milliroentgens? Please correct me if I am wrong here...

I al looking to purchase at least 1 low range/dose Quartz Fibre
Dosimeter(s), if anyone can help in the supply of 1 or 2 that are of
the same design as the ones in the photo so that they can be charged
using my original Stephen Universal Quartz Fibre Dosimeter charger
(as per the photo) and their range is 0 - 0.2r or less.

Happy new year and thanks in anticipation.
Keith Watt RN (Rtd.)

#141 From: "Geo>K0FF" <GEOelectronics@...>
Date: Sat Jan 5, 2008 3:48 pm
Subject: Check Spots continued
k0ff
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If the check spot contains only "Radium D+E" i.e. Pb-210 or radiolead, it has a half life of 22 years so the readings will be less over time. It is
predictable and can be accounted for. Such spots installed in 1962 would be about 2 half-live decayed by now or ~1/4 of the original activity.
 
If the check spot uses radium or any type of uranium, there is no appreciable decay in the reading over time.
 
Some Russian units use Sr-90 as do certain American ion-chamber units, as well as Kr-85 and other isotopes. Each of these
would have to have their reading recalculated according to their individual half-lives.
 
Depending on the probe and the CPM rate, an isotope that is 1/2 as strong as the original may not read exactly 1/2 the CPM, due to
dead-time issues in the probe.
 
Geo

#140 From: "Geo>K0FF" <GEOelectronics@...>
Date: Sat Jan 5, 2008 3:30 pm
Subject: Check Spots.
k0ff
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Please refer to the decay chain for U-238 on page 2 of this chart,
if you do not have one printed already:

http://www.ead.anl.gov/pub/doc/natural-decay-series.pdf


Going down the chain, looking at only Gamma energies right now, with
a computerized-spectrum analyzer, the SpecTech UCS-30 and a 3" X 3" sodium iodide detector.

At the top >U-238. The parent of this decay chain. Other decay chains
are headed by Th-232 and U-235. Any isotope removed by man or nature from
a chain,will be considered the head of it's own chain, as in Radium , Radon,
or even Radium D+E.>
Right at the top there is an X-ray at 100 keV and Gammas at 185, 766
and 1001 from the Pa-234m. If these are present, parent U-238 is
present, and by default all the other lower daughters should be there, if they have not been removed by
man or nature ( Radon is a gas, it can fall away, being heavier than air,
disturbing the lower part of the chain)
Pictures of this and all the other graphs can be seen at:

http://groups.yahoo.com/group/GeigerCounterEnthusiasts/files/
Look at the far left side for those telltale energies from the higher
parents.

All the graphs will show some Gamma from K-40 at 1460 keV. This is
not from the test sample, but part of the background radiation here at my place. Some
of it may even be my own bones (see graph of chicken bones later on!).

Down the chain is Radium 226, a strong alpha emitter, with a weak
Gamma, which is undetectable by my home lab setup. The Alphas of course are
easy to detect, but hard to tell from other Alphas generated later down the
chain.
Radium was first refined over 100 years ago. When it is removed
that way from the surrounding U238 parent, it starts it's own decay chain,
which is simply a continuation everything below it on this chain.

Pb-214, or " Radium B" is quite detectable with a Gamma
Scintillator, with a striking 351 keV Gamma. Likewise "Radium C" also known as Bismuth-214,
which is the next in line of decay. It has a 609 keV, 1112 keV and a 1760 (unique) keV Gamma.
If these two are present, then parent Radium-226 is present. ( The
letter designators are little used any more, scientists simply call an
isotope by it's name and weight)


Way down near the bottom is Radium D+E. Today known as Lead-210
(radiolead) and Bismuth-210. No Gammas detectable from these, but you know they
must be in the mix if the higher members are present. Lots of Betas though.
It is possible that D+E alone have been removed, and used in a test
spot, easy to determine, simply by the absence of Gammas from the higher
members Pb-214/Bi-214.

So by logic:
Got Betas, no Gamma?= Radium D+E only. Black, crumbly

Got Betas + 1760 keV Gamma (Bi-214) but no 100k X-Ray or Pa-234
Gammas?= Radium-226

Got Betas+1760 Gamma + 100k X-Ray and the Pa-234 Gammas?= Uranium-238. Grey, hard

Has the U-235 been removed from natural Uranium, a.k.a. DU? The presence or absence of a 185 keV peak easily determines the
state of U-235 in a sample.
DU metal and U oxide are way different creatures, physically. DU
metal is used in ammo yes, but also for it's density and weight value in airliners, ocean
liners and sailboats as ballast.
Last winter I handled and measured a big chunk of the stuff at White
Sands Missile range. Pretty radioactive according to my pocket Geiger, and
not just Alphas, as it was in a plastic bag.


Now on the CDV 700 test spots.

Anton= Radium-226. Why ? Because it has the Pb-214 and Bi-214 that are
present
when Radium 226 is the parent. Further, there are no higher Gammas
from the
Pa-234, ruling out a higher parent. This is the only metallic
appearing
material I have seen, I assume electroplated(?).
Spectrum available in the above mentioned files.

Anton's books state D+E. Why this is I don't know. It's true D+E are
in
there, they have to be, as they are the lower decay daughters. Their
D+E
will not deteriorate though,as it is continuously replenished by the
Radium-226. Perhaps not all the Anton's have the
metal foil. The only 2 I ever opened did, one was a model 5, on a
model 6.

ENi 6B: some books say Radium D+E some books say Uranium. All have
tested
here
are D+E. Many of the ENi's I've seen ( maybe 100?) have deteriorated
activity from the test spot ( 21/2 half-lives old now after all)
Update:
Some ENI's have normal 2+ "mR" strength test spots, but seem to have
been
tampered with. Perhaps in some programs, they were renewed at some
point.
(Geo)


Victoreen Instruments: CDV 700 books for 6, 6A and 6B say "Beta
Source".Vic
491 book says Uranium. In fact, by measurement, some are natural
Uranium,
theses have a hard dark gray brittle material. The majority I've
tested are
the black crumbly stuff,
D+E. From Bill Kolb, author of "Living with radiation":
From: "William Kolb" <analemma@...>
To: "'K0FF'" <K0FF@...>

>George,
> The Victoreen Cutie Pie used natural uranium for its check source.
It is
> primarily a beta emitter but you will see lines just below 100KeV
(U-K
> xrays), at 185KeV (Pa-234), 766KeV (Pa-234m) and 1001KeV (Pa-234m).
The
> Nuclear Chicago Cutie Pie had a C-14 beta source. As far as I know,
> Victoreen only used natural uranium on its meters, including the
> CDV-700s.
>
> bill
>


PRI books say Uranium Ore for the 106B, and "calibrated Radium" for
the
107B, 109, 110, 111B, 111C. Look at the PRI spots in the dark, some
glow!

Lionel definitely D+E....no Gammas present, just the Betas.


Just a reminder that any Alphas present in a covered sample will be
filtered
out by the covering material. Only Beta and Gamma can escape the
cover material.
 
 
 
With simple equipment, Alphas,Betas, Gammas can be determined. Using a pancake
probe, Alphas are filtered out using a 3X5 card or even a piece of typing paper. Betas are filtered out
with a 3mm thick aluminum sheet or 1/2" Plexiglas.
 


Have Fun

Geo

#139 From: "Geo>K0FF" <GEOelectronics@...>
Date: Sat Dec 29, 2007 10:49 pm
Subject: Scintillator PREAMP- Make ANY Geiger a SCINTILLOMETER
k0ff
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350010924496
 
Pictures on there now. Schematics in FILES for home construction project.
 
Also more info at:
 
have fun
 
Geo

#138 From: "Geo>K0FF" <GEOelectronics@...>
Date: Mon Dec 24, 2007 6:01 pm
Subject: Thorium welding electrodes, mantle dust etc.
k0ff
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Natural Thorium 232 is abundant in the environment. As an industrial material thorium has been used to enhance a
great number of products. Because all thorium isotopes are radioactive, non radioactive substitutes like cerium have been employed, with a certain degrading of the original specifications. In some applications, only thorium can perform, such as filaments for high power radio transmitting tubes. .
 
The comments below were in relation to thoriated TIG welding electrodes but applies to thorium in general. Usually thorium is supplied in an oxide or nitrate, but pure thorium metal exists ( very expensive!!).
 

 
Depending on how long ago the thorium 232  was refined, it will contain more or less of its decay products also. Freshly refined Thorium would be thorium metal only if the process is efficient. This includes both the Th-232 parent and the Th-228 decay product, since all isotopes of the same element are indistinguishable in chemical reactions.
 
The Th-228 would promptly regenerate all the lower decay products, which include radium radon, polonium(s),radio-lead,radio-bismuth and thallium-208*.
 
Soon after refining, a few years, the Th-232 parent will regenerate the upper members of the decay chain which includes radium, Ac-2228 and Th-228.
 
When burned or ground up on a grinder, the electrode would release these various elements into the environment, including the radon , which is a gas.
 
Each element will continue to go through radioactive decay, transmuting to the next element in the chain. Each individual element can be considered a parent of its own decay chain. All will eventually end up as stable Lead (Pb) -208.
 
 
More than you wanted or needed to know probably, but some of us spend a great deal of time trying to identify each and every one of these elements individually, as a hobby.
 
 
Although it takes specialized equipment, rudimentary tests can be done with only a pancake probe, a paper card, and a piece of aluminum sheet. Application of the card over the face of the detector removes the alpha particles, application of the aluminum sheet ( 3mm) removes the alphas plus the betas.
Simple arithmetic reveals the alpha, beta and gamma components.
 
* Tl-208's gamma of 2.62 MeV is used to verify the presence of thorium in ore, as it is a unique energy signature.
 
Have fun
 
Geo
 
 
 
 
 


#137 From: "John Richards" <cyclojohn@...>
Date: Fri Dec 21, 2007 1:55 am
Subject: Radioactive Boy Scout - Sentenced
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Geo:

Yes, it is not a good idea to take apart smoke Detectors, a recent
site suggested using the source for a homemade Spinthariscope - since
it is an Alpha emmitter, failing to mention its Gamma components...
(Australian site, I think)


Anyway, the Radioactive  Boy Scout was Sentenced to 90 days

http://www.foxnews.com/story/0,2933,299362,00.html

http://en.wikipedia.org/wiki/David_Hahn

History:
http://www.abc.net.au/science/k2/moments/s595641.htm

http://www.dangerouslaboratories.org/radscout.html

Enjoy,

John-

#136 From: "Geo>K0FF" <GEOelectronics@...>
Date: Wed Nov 28, 2007 1:23 am
Subject: Testing for lead in paint using radiation.
k0ff
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Testing for lead in paint and other products using radiation.

 

There is a lot of squawking going on concerning China imports containing lead in  paint, especially on children's toys, and rightfully so.

Decades ago, we in the U.S. used lead in many products, including gasoline and paint, now banned. As a resident of Missouri, a big lead mining and processing state I am particularly keen on the subject of detecting lead where it should not be. It should probably be mentioned that some of my former clients were St. Joe Lead, National Lead ( NL Industries), and Ethyl Corp.

 

All atoms are made up of nucleons and electrons. When an electron is removed from an inner shell, it must be replaced by another electron to maintain stability in the atom. In atoms heavier than hydrogen, this action releases energy, in the form of X-Rays. There are several sources from which the missing electron may be replaced, and in heavy atoms, there are other shells from which the electron may go missing.

We will concentrate on the innermost electron shell, called the K shell. Extra energy introduced into the atom by using an X-Ray source, Gamma source, a Beta or other charged particle source, can cause the K electron to gain energy, and leave the shell, heading off to parts unknown at great speeds. As mentioned this space must be filled, if from the L shell, this reaction is called  K-alpha. If it gets replaced by the M shell, we call that K-beta and this reaction has a different energy.

 

Most elements fill the K shell hole from the L shell, giving rise to a distinct X-Ray, unique to that element, called the "K-alpha CHARACTERISTIC X-RAY ENERGY"

 

For lead (Pb) this K-a energy is 74.96 keV.

 

The procedure is simple, excite the material under test with an X-Ray tube or isotope  whose energy level is substantially higher that 74.96 keV. Then at the same time, scan the DUT (Device Under Test) for the tell-tale 74.96 keV emission. Apparatus are available to do all the needed functions such as:

http://www.niton.com/Lead-Paint-Testing/Applications/beyond-lead-paint.aspx

http://www.rmd-lpa1.com/

Many apparatus variants exist, as mentioned, using protons, beta particles, Cd-109 and Fe-55, Co-57,  as well as Am-241 as the excitation source. Virtually any element can be examined using this X-Ray Fluorescence method, except hydrogen. The acronym PIXE (Particle Induced X-Ray Emission) is applied if the excitation source is a charged particle. I have read of Alpha Particle excitation but have never been able to verify that personally.

 

Making the element X-Ray Fluorescence is very easy, I use a simple Kr-85 beta source and test jig. Detecting the characteristic X-Ray is a bit more problematic in lighter atoms, due to the low energies involved.  HPGE probe, CdTe, even Mercuric Iodide probes are preferred, but many NaI(Tl) give great results with the heavier elements. Virtually ANY detector will pick up the 74.96 keV from Pb.

 

Of course a Gamma Spectrum Analyzer (MCA) is required to read the exact energy, but the simplest SCA's will work too. System calibration is easy by using Am-241's 59.5 keV and 88 keV from Cd-109 as standards.

 

Lead's 74.96 X-Rays can be exited by Cosmic Rays too. For this reason and others, when we shield a probe in the lab, we use a lot of lead, but then shield the lead with tin or cadmium, then shield that with copper. Such a "graded shield", if built with pre WW2  or ancient lead, will make an exceptionally effective probe shield. The shield for my 3" X 3" probe is 300+ pounds, the one for my Marinelli Beaker probe is well over 1000 lbs. A BIG one would run nearer to 3000 lbs.

XRF can obviously scan for the other restricted ROHS elements, Hg, Cd, Cr, Br,

Compact, portable instruments are costly, can run 20,000 USD easily. There is no excuse for Corporate HQ at Wal-Mart, Mattel, et.al. not having ONE unit and someone who knows how to use it.

Lab setups can be significantly more expensive, but at what cost compared to company brands like Mattel losing all?

 

Below is an amateur lead XRF detector system, all home made from commercial components.

 

Pb XRF on Gamma Spectrum Analyzer

 

Setup: 2" NaI well scintillator with thin side sections. Known to be OK with
low energy Gammas, but not optimized for this service- calibrated with
Cs-137. Home made base and dynode string, single coax feed. Adapted to 2
coax instrumentation via a home made splitter box.
Spectrum Analyzer is SpecTech UCS-20, USB connected to an HP laptop.
Source = 4 uCi Kr-85, Betas blocked from direct interaction with probe by a
stack of 3x5 cards. Distance from source to detector= 4".
Thin lead foil used in second step, in transmission mode to stimulate
X-Rays.
Foil approx 3 mils thick. Can't be sure because it has a thin plastic
coating which I can't remove. Laminate total thickness is 4 mils. Experiment
set up so plastic is away from the Beta source, with the Betas striking bare
lead foil. X-Rays must penetrate the plastic on way to probe, so some
attenuation anticipated.

Charts
1: Spectrum chart showing Kr-85 only. Note nice peak at 514 keV which is the
characteristic Gamma for Krypton-85. The Beta Rays are not detectable directly by this probe, only the resultant X-Rays.


 

2: Add thin section of lead foil in ray path. Note same 514 keV but now also
a sharp peak at 75 keV, the characteristic K Shell X-Ray for Pb.


 

3: Lead spectrum and no lead spectrum overlaid. 514 same on both.


 

4: Spectrums numerically cancelled, known as background stripping, showing
only the difference, which is the 75 keV peak, and the other lesser low
energy products.


Another time I'll try the same experiment with reflection instead of
transmission mode, and try Sr-90 and other isotopes to energize the lead.
Even Gamma sources should be able to do the trick.

 

UPDATE- This article was first printed in winter of 2004. Since then my setup has improved drastically. I still use the same old exempt quantity Krypton 85 source though, it wound up being the best of all. Most of the improvements in this system were to the probe shield and the probe itself was upgraded a notch to a 3" X 3" Bicron NaI(Tl), pretty much the standard lab probe I think.

Have Fun

 

Geo

 

 

 

 


#135 From: "Geo>K0FF" <GEOelectronics@...>
Date: Tue Nov 27, 2007 9:56 pm
Subject: New spectrometer apparatus
k0ff
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For the Home Lab:
 
 
Some of the experiments possible with this are:
X-Ray diffraction
Bragg reflection
Spark Gap
Rectilinear propagation
Inverse Square Law
Half and Tenth Value Thickness
Scattering
Moseley's Law
 
There are 38 formal experiments in the lab manual, which I will post in FILES at
 
 
Many of these lab experiments can be done using common apparatus and jigs.
 
Have fun
 
Geo
 

#134 From: "Bill Coon" <kc8lrm@...>
Date: Mon Nov 12, 2007 10:33 pm
Subject: uses of a Tritium Self Luminous Exit Sign
kc8lrm
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Hi,
     Dug out my 20 year old self luminous exit sign and found it still
luminescent and fully quiet - no counts of any kind. It's a totally
sealed unit, appears to be seam welded plastic.
     Does this unit have and experimental use? Or just a curiosity?

Thanks

#132 From: "Steve Schoner" <schoner@...>
Date: Fri Oct 26, 2007 3:57 am
Subject: Re: [CDV700CLUB] Radioactive tubes
steve_schoner
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A brief list can be found here:

http://tubecollector.org/documents/radioactive.htm

Not all tubes are still radioactive now, if they have short lived isotopes.

Thorium charged tubes are just barely above background.  But the ones with
radium are quite hot and will be for thousands of years.

Steve.




Please note: message attached

Anybody have or know the location of a list of electron tubes with radioactive elements?




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#130 From: "Geo>K0FF" <GEOelectronics@...>
Date: Wed Oct 17, 2007 5:42 pm
Subject: For Sale CDV-715 Geiger Counter. WORKS- Passes CIRCUIT CHECK!!
k0ff
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Subject: For Sale CDV-715 Geiger Counter. WORKS- Passes CIRCUIT CHECK!!

THIS IS A CDV-715 Geiger Counter
 
THIS IS A CDV-715 GEIGER COUNTER PASSING CIRCUIT CHECK
 
ANY QUESTIONS?
 
 
 
 
 
 
if so read this:
 
Geo

#128 From: "Geo>K0FF" <GEOelectronics@...>
Date: Sun Oct 14, 2007 3:12 pm
Subject: Radioactive Trilobite
k0ff
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Added to the file, a rather nice radioactive (shows Ra-226 daughters) Trilobite fossil that I
collected in Morocco on 1994/1995 field trip.
 
 
The rock to the right is the overburden, the part of the rock that covered the trilobite and helped
created the fossil. It's rare to come back with such a nice pair, fitting together perfectly like a jigsaw puzzle.
 
From the Paleozoic Eratrilobites went extinct in the Great Permian Extinction, 251,000,005 years ago
before the dinosaurs arose.
 
Have fun
 
Geo

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