I am trying to analyze zoledronate in serum by derivatizing it to its ethyl ester and then analyzing by GC-MS,however,the internal standard used in the article...
These links will have the information you need. 600E pump: http://www.waters.com/WatersDivision/SiteSearch/AppLibDetails.asp?LibNum=720000751EN 490E detector: ...
Dear Friends, I am using an old Varian 3400 GC (with FID detector; there is no slip injector). I am injecting 1 ul of sample (in pentane/hexane). It is giving...
If your samples are soluble in it, you can try carbon disulfide, CS2. The FID is almost 'blind' to this solvent, keeping a low steady baseline. You will need...
Dear Members, I wanted to fill SS column with C 18 material.Does any one can help me as how to fill the column or give me a clean procudure guidelines,The...
Rajesh Galgalikar
rajesh@...
Jul 7, 2006 12:23 pm
2280
... You didn't say, but I'll assume you're using a common capillary column. Check your split ratio. It sounds like you're running a splitless injection, so...
David Bostwick
david.bostwick@...
Jul 7, 2006 2:38 pm
2281
I want to find k and alpha for poly(ethylen)glycole adipate in chlorophorm to make some GPC measurements. Can somebody help me? A.T ... Yahoo! Messenger with...
Dear members of this forum, Thanks for all owing to many members gave the information I need in order to finish my work. Thanks as always again, Diego ... ...
Diego Delmonte
tequila2@...
Jul 19, 2006 1:25 am
2283
Dear colleagues, I'm needing some help again! I need 2 articles that I don't have access. Can somebody send them to me? 1: Lapolla A, Flamini R, Dalla...
Anyone have a good method for caffeine (or other markers of human sewage) in river water? Preferrably SPE HPLC but GCMS could work also. The more detailed...
Hi, we are currently testing a batch of alpha terpineole (FCC). The requirement for the assay is: not less than 96.0% (sum of alpha-, (E)-beta-, (Z)-beta-,...
Thomas Vater
thomas.vater@...
Dec 2, 2006 9:47 am
2286
11th December 2006 Dear colleagues, I would like a copy of the following article if any of you have it in your research library: Parpinello, Giuseppina Paola;...
Tony_Herlt
herlt@...
Dec 11, 2006 1:07 am
2287
Dear members of this list, I would appreciate if anyone help me in order to get two articles which is very helpfull for me in order to improve my work with ...
tequila2@...
Dec 15, 2006 11:35 am
2288
Senior Scientist/Group Leader - Analytical Development A great company in Tarrytown, NY is seeking a Senior Scientist/Group Leader-Analytical Development....
Hello, I'm working on an HPLC, Hewlett Packard 1050. I'm not being able to detect any peak, even though I can see that the detector is reading an absorbance...
Manager, Process Development - San Diego, CA A client of ours in San Diego, CA is seeking a Manager, Process Development. They are a specialty biotechnology...
Dear members of the list, i have been appointed to a new laboratory and i am expected to learn how to detect mycotoxins in food and feed materials. firstly i...
Senior Analytical Scientist - Torrance, CA I am assisting to recruit a Sr Analytical Scientist for a great company in Torrance, CA. Would you be interested in...
dear members of the list, i am looking for a training program for mycotoxin analysis by using biosensors. would someone lead me an addres to solve my problem? ...
I'm running some HPLC soybeans extracts with ETOH 70% with acetic acid 0,1%, but I got no Genistein peak, although I got a peak at gradient run at 37 minutes...
Hi, Is the system conected to an integrator or to a chromatography station? In either case I would first check to see if the cables are connected tightly. Do...
the shifflet's
shiffty@...
Feb 24, 2007 12:44 pm
2296
26th February 2006 Dear colleagues, I am trying to obtain the following article: Title: Analysis of peptides at low levels using a chromatography system...
Tony_Herlt
herlt@...
Feb 25, 2007 10:18 pm
2297
I need the components of a simple method to determine Vitamine 25 OH D3 in HPLC.The method is as follow: Sample preparation Mix briefly 500 µl serum/plasma...
Dear Friends Could you anyone suggest us for doing Chef test and swap test in water,meat and fish. Charm sciences inc is making such instrument. If you know...
We have a HP5890 GC-FID and a Varian 3400 GC-ECD. Both currently have integrators. I'd like to replace both integrators with one computer. We never use both...
3rd May 2007 There is chromatography data system software called Delta 5.5 that would probably work well with your GC instruments and is competitively priced. ...
Tony_Herlt
herlt@...
May 2, 2007 11:29 pm
2302
Problem: We are consistently seeing peak(s) around 14-18 amu over 40 abundance in the autotune spectra on an Agilent 5973 MSD connected to an Agilent 6890 GC....
Why a C18 Column with a mobile phase with ion pairing conditions on more time than a C18 with a mobile phase without ion pairing? thank you Gianfranco ...
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