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Re: (unknown)   Message List  
Reply | Forward Message #273 of 284 |
Re: [spectroscopy] (unknown)

Oh!  I thought you wanted all the H's to be D's.  If it is just the hydroxyl D that you want, just start with an alkyl halide and either treat it by heating with NaOD or KOD in D2O or even just do it in gas phase with D2O and R-X heated under some pressure.  The analogous reactions for hydrogen, to make R-OH from R-X are well known, see any textbook.  And again, when you finally do get product you can write this up and publish it.  Then people can refer to your work and yhou will be in all the footnotes.
Bill


In a message dated 3/17/05 8:30:46 AM Pacific Standard Time, vandanas@... writes:


I didn't ask the process of denaturing. I wanted to know the procedure of
making deuterated ethanol (C2H5OD).





Thu Mar 17, 2005 5:29 pm

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CatalyticChemist@...
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Forward 		Message #273 of 284 |
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Dear Vandana My name is Barbara and I am the wife of Richard Payling whose website is thespectroscopynet.com. I regret to inform you that Richard died whilst... 		Designer1
gd_oes
Offline Send Email 		Apr 15, 2004
7:38 pm

Please contact Thomas Nelis about this. Barbara Hoving ... From: Vandana Sharma To: Spectroscopy Sent: Sunday, March 28, 2004 3:40 PM Subject: [spectroscopy]...
Designer1
gd_oes
Offline Send Email 		Jun 3, 2004
10:43 am

Hi, I think a drop of metanol is enough to denature the etanol. urs Varatharajan. Vandana Sharma <vandanas@...> wrote: Hello all, Does any body know...
varathu rajan
varachem2001
Offline Send Email 		Mar 16, 2005
4:35 pm

Hi Varathu, I didn't ask the process of denaturing. I wanted to know the procedure of making deuterated ethanol (C2H5OD). Regards, Vandana ...
Vandana Sharma
vandypph
Offline Send Email 		Mar 17, 2005
4:18 pm

Oh! I thought you wanted all the H's to be D's. If it is just the hydroxyl D that you want, just start with an alkyl halide and either treat it by heating...
CatalyticChemist@...
Send Email 		Mar 17, 2005
5:29 pm
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